Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | Sodium 3-hydroxyacrylonitrile | HCID 86738287 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70549270 | HCID 70549270 | 79.6% |
Reaction Steps
32.5 g (0.25 mol) of sodium-3-hydroxyacrylonitrile (content 70%) is added to a mixture of 17.8 g (0.25 mol) of pyrrolidine, 12.3 g (0.125 mol) of sulfuric acid and 200 ml of ethanol, and the mixture is stirred at 50° C. for 7 h. After working up as in Example 50, 24.3 g of 3-pyrrolidine acrylonitrile (79.6%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04319024 |
|---|
| Source dataset | uspto-grants-1982_03 |
|---|
| ORD ID | ord-f4ff8d10492346a7bd980617bc8eed74 |
|---|
| Source note | uspto-grants-1982_03 |
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