HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | HCID 2734036 | HCID 2734036 | — |
| Product | HCID 13037485 | HCID 13037485 | 14.5% |
Reaction Steps
The procedure of Example 1 was employed utilizing N-benzylaniline and cyclohexyl phosphonic dichloride. The crude product produced as a result of the chromatographic separation yielded without additional purification 1-cyclohexyl-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (2.7 g, 14.5% yield) as a beige solid having a melting point of 167°-169° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-f3b877a608ae4d9ca86d336cdbaa71e5 |
| Source note | uspto-grants-1982_03 |