HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | HCID 20548444 | HCID 20548444 | — |
| Product | HCID 13037487 | HCID 13037487 | 66% |
Reaction Steps
The procedure of Example 1 was employed utilizing N-benzylaniline and 2,4-dimethoxyphenyl phosphonic dichloride. The reaction of the dilithio compound and the 2,4-dimethoxyphenyl phosphonic dichloride was conducted at -76° C. to yield 1-(2,4-dimethoxyphenyl)-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (7.2 g, 66% yield) as a white solid having a melting point of 173°-175° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-4c65926bfefc45829776e43438c2d45b |
| Source note | uspto-grants-1982_03 |