HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | HCID 12670627 | HCID 12670627 | — |
| Product | HCID 13037494 | HCID 13037494 | 27% |
Reaction Steps
The procedure of Example 1 was employed utilizing N-benzylaniline and 3-methoxyphenyl phosphonic dichloride. The reaction of the dilithio compound and the 3-methoxyphenyl phosphonic dichloride was conducted at 0° C. to yield 1-(3-methoxyphenyl)-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (2.75 g, 27% yield) as a solid having a melting point of 170°-172° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-20a24870317c4040b8e909fd1fafa834 |
| Source note | uspto-grants-1982_03 |