HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | Phosphonic dichloride, (2-methylphenyl)- | HCID 10921725 | — |
| Product | HCID 13037495 | HCID 13037495 | 8% |
Reaction Steps
The procedure of Example 1 was employed utilizing N-benzylaniline and 2-methylphenyl phosphonic dichloride. The reaction of the dilithio compound and the 2-methylphenyl phosphonic dichloride was conducted at 0° C. to yield 1-(2-methylphenyl)-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (0.8 g, 8% yield) as a yellow solid having a melting point of 181°-183° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-566fa30f635046999e9165701f1e645b |
| Source note | uspto-grants-1982_03 |