HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | (4-Fluorophenyl)phosphonic dichloride | HCID 12670632 | — |
| Product | HCID 13037506 | HCID 13037506 | 30% |
Reaction Steps
The procedure of Example 26 was employed utilizing N-benzylaniline and 4-fluorophenyl phosphonic dichloride to yield a pale yellow solid. The yellow solid was recrystallized from ethyl acetate to yield 1-(4-fluorophenyl)-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (5.9 g, 30% yield) as white needles having a melting point of 119°-120° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-dcc07b202940428cb8ba73153129951c |
| Source note | uspto-grants-1982_03 |