HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | Phosphonic dichloride, (p-methoxyphenyl)- | HCID 216711 | — |
| Product | HCID 13037507 | HCID 13037507 | 7% |
Reaction Steps
The procedure of Example 26 was employed utilizing N-benzylaniline and 4-methoxyphenyl phosphonic dichloride to yield 1-(4-methoxyphenyl)-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (0.7 g, 7% yield) as a white solid having a melting point of 190°-192° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-25ebc9b8bd5b4b909ada084517fb828b |
| Source note | uspto-grants-1982_03 |