HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylaniline → HCID 13037519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylaniline | HCID 66028 | — |
| Reactant | HCID 12670629 | HCID 12670629 | — |
| Product | HCID 13037519 | HCID 13037519 | 4% |
Reaction Steps
The procedure of Example 38 was employed utilizing N-benzylaniline and 4-trifluoromethylphenyl phosphonic dichloride. The crude product produced as a result of the chromatographic separation was crystallized from diethyl ether and petroleum ether and recrystallized from diethyl ether to yield 1-[4-(trifluoromethyl)phenyl]-2-phenyl-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (0.5 g, 4% yield) having a melting point of 187°-189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04319913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-c8a6001e2b4e486bbe9b72442fc26a7d |
| Source note | uspto-grants-1982_03 |