HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → o-CRESYL GLYCIDYL ETHER
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Catalyst | Piperidine | HCID 8082 | — |
| Product | o-CRESYL GLYCIDYL ETHER | HCID 16640 | — |
Reaction Steps
A solution of ortho-cresol (64.8 g., 0.6 mole), epichlorohydrin (330 g., 3.6 mole), and piperidine (5 drops) was allowed to react and the product was isolated using the same methods outlined hereinabove in Example 1. Concentration of the methylene chloride extract gave 95 g. of crude epoxide (IIb) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321398 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-90a8cd89dff7435b90f89e7d01cc8385 |
| Source note | uspto-grants-1982_03 |