HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphine, tris(4-methylphenyl)- → HCID 10855191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphine, tris(4-methylphenyl)- | HCID 13956 | — |
| Reactant | Ruthenium trichloride hydrate | HCID 6093376 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10855191 | HCID 10855191 | — |
Reaction Steps
Using the procedure of Example 1, 50 mls. of methanol, 6.0 grams of tri-paratolylphosphine and 1.0 gram of ruthenium trichloride hydrate are stirred and heated at reflux under nitrogen for 24 hours to form tris(tri-paratolylphosphine) ruthenium dichloride as an insoluble powder which is recovered by filtration (4.2 grams).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04321414 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-a37b42f07d0f45a8b752e9bb879d634d |
| Source note | uspto-grants-1982_03 |