HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 12960032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 12960031 | HCID 12960031 | — |
| Reactant | HCID 54142171 | HCID 54142171 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12960032 | HCID 12960032 | — |
Reaction Steps
3-(4-Biphenylyl)-3-methoxyacrylonitrile plus 3-(4-biphenylyl)-3,3-dimethoxypropionitrile (2.9 grams as a mixture from example 6), hydroxylamine hydrochloride (4.7 grams), and sodium methoxide (11.9 grams) were mixed in 500 ml. of methanol and refluxed for 48 hours. After the methanol was evaporated, water was added and the product, separated by filtration, yielded 1.2 grams. NMR confirmed the identity of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322429 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-7b496d828ed1407b8fb38fa3b051e77b |
| Source note | uspto-grants-1982_03 |