HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzoyl chloride → HCID 13035562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzoyl chloride | HCID 78392 | — |
| Reactant | JR-9574, 5-(4-Chlorophenyl)isoxazol-3-amine, 97% | HCID 13035539 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13035562 | HCID 13035562 | — |
Reaction Steps
5-(4-Chlorophenyl)-3-aminoisoxazole (400 milligrams prepared according to the teaching of Examples 11-14) was added to 2,6-dichlorobenzoylchloride (430 milligrams) in 50 ml. toluene and refluxed for 48 hours. The solvent was then evaporated and ethyl alcohol added; upon subsequent heating and filtering the bis acylated product was recovered; m.p. 219°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322429 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-eb3fd644dbe54897b09eff30d1dcb86d |
| Source note | uspto-grants-1982_03 |