HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzoyl chloride → 2,6-Dichloro-N-(3-benzisoxazolyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzoyl chloride | HCID 78392 | — |
| Reactant | 1,2-Benzoxazol-3-amine | HCID 2779749 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,6-Dichloro-N-(3-benzisoxazolyl)benzamide | HCID 20546754 | — |
Reaction Steps
3-Aminobenzisoxazole (2 gram), 2,6-dichlorobenzoylchloride (2 gram), and 50 ml. of toluene are heated at reflux for 16 hours. After evaporation of the solvent at reduced pressure, the resultant oily semi-solid is triturated with ether. The solid so formed is then washed with ether and water and constitutes the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322429 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-4944d88c8d17409192df679111a9782c |
| Source note | uspto-grants-1982_03 |