HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzoyl chloride → HCID 20546750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzoyl chloride | HCID 78392 | — |
| Reactant | 7-Trifluoromethyl-benzo[d]isoxazol-3-ylamine | HCID 10774456 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20546750 | HCID 20546750 | — |
Reaction Steps
7-(Trifluoromethyl)-3-aminobenzisoxazole (2 gram), 2,6-dichlorobenzoylchloride (2 gram), and 50 ml. of toluene are heated at reflux for 16 hours. After evaporation of the solvent at reduced pressure, the resultant oily semi-solid is triturated with ether. The solid so formed is then washed with ether and water and constitutes the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322429 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-040ca746202f4b7a9c02a29f90e9d7e2 |
| Source note | uspto-grants-1982_03 |