HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 20545910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 20545898 | HCID 20545898 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20545910 | HCID 20545910 | 93% |
Reaction Steps
A mixture of 4(4-chlorophenyl)-7-hydroxy-2,2-dimethyl-1-tetralone (17.6 g), epichlorohydrin (30 ml) and potassium carbonate (6.0 g) was heated under reflux in acetone (30 ml) for 24 hr. The hot mixture was filtered and evaporation of the filtrate in vacuo gave 4-(4-chlorphenyl)-7-(2,3-epoxypropoxy)-2,2-dimethyl-1-tetralone as a light yellow gum (8.4 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322370 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-6e381eb75c73498691977b0a71a746c2 |
| Source note | uspto-grants-1982_03 |