HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 13035114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Heptane | HCID 8900 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 13035115 | HCID 13035115 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13035114 | HCID 13035114 | — |
Reaction Steps
To 6.3 gram NaHCO3 (0.075 mole) dissolved in 75 ml water was added a mixture 50 ml of heptane and 25 ml MeCl2. To the agitated 2-phase system was added 12.2 gram D(-) phenylglycine butyl ester hydrochloride (0.05 mole) over 20 minutes at 12°-14° C. The layers were allowed to settle.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322548 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-09c819806b644e8fa262f588778821fb |
| Source note | uspto-grants-1982_03 |