反应详情

To 6.3 gram NaHCO3 (0.075 mole) dissolved in 75 ml water was added a mixture 50 ml of heptane and 25 ml MeCl2. To the agitated 2-phase system was added 12.2 gram D(-) phenylglycine butyl ester hydrochloride (0.05 mole) over 20 minutes at 12°-14° C. The layers were allowed to settle.