HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13037120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 1-Chloro-3-phenoxy-2-propanol | HCID 94300 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13037120 | HCID 13037120 | — |
Reaction Steps
A mixture of 55 g (0.29 mol) of 1-chloro-2-hydroxy-3-phenoxypropane, 170 g (1.1 mol) sodium iodide in 1.0 of acetone is refluxed in the dark under a nitrogen atmosphere for 3 days. The acetone is removed in vacuo, the residue slurried in chloroform, filtered and the filtrate stripped to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04322557 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-b7314cbcc7e3438baf97e853cebd289e |
| Source note | uspto-grants-1982_03 |