HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 69079036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | HCID 69082365 | HCID 69082365 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69079036 | HCID 69079036 | — |
Reaction Steps
The product of Step A (5.01 g, 17.5 mmol) in THF (30 mL) was treated to dimethylformamide dimethylacetal (4.97 mL, 35.0 mmol, 94% assay) at 60° C. for about an hour. The reaction was concentrated and used directly in Step C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278304B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-b0097ade3fdc4160a8c312cd7c524e4e |
| Source note | uspto-grants-2012_10 |