HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57989597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57989587 | HCID 57989587 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57989597 | HCID 57989597 | — |
Reaction Steps
TFA (1.5 ml) was added to a cooled (0° C.) solution of (S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)indolin-2-yl)methoxy)acetate (0.5 mmol) in DCM (6 ml) and the mixture was stirred for 2 h at room temperature. The solvent was removed under vacuum and the residue used in the subsequent stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278319B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-894bb953def5409ba4d05001bc6fda38 |
| Source note | uspto-grants-2012_10 |