HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 68802039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Dimethylaminomethyl-5-trifluoromethoxy-indan-1-one hydrochloride | HCID 69450781 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68802039 | HCID 68802039 | — |
Reaction Steps
14 g of the product from step 3 were dissolved in water; the solution was adjusted to pH 12 with 32% sodium hydroxide solution, while cooling with ice, and extracted three times with dichloromethane, and the combined organic phases were dried over magnesium sulfate, filtered and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278338B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-778622f470074d93814ea356c2bf25bd |
| Source note | uspto-grants-2012_10 |