Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pentanal | HCID 8063 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | Ethyl 2-oxo-3-phenylpropanoate | HCID 12292599 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57923948 | HCID 57923948 | — |
Reaction Steps
3-Imidazol-1-yl-propylamine (1 mmol) and pentanal (1 mmol) were added to ethanol (5 ml). After 30 min 2-Oxo-3-phenyl-propionic acid ethylester (1 mmol) was added. The reaction was heated to 50° C. and stirred for 24 h. After evaporation of the solvent the residue was purified with chromatographic methods.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08278345B2 |
|---|
| Source dataset | uspto-grants-2012_10 |
|---|
| ORD ID | ord-7ee580f2e2c74e03bc97980480a1fb53 |
|---|
| Source note | uspto-grants-2012_10 |
|---|
