Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 5-Methylfurfural | HCID 12097 | — |
| Reactant | Ethyl 2,4-dioxoheptanoate | HCID 3006750 | — |
| Reactant | HCID 178507353 | HCID 178507353 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178450348 | HCID 178450348 | — |
Reaction Steps
1H-Benzoimidazol-5-ylamine (1 mmol) and 5-Methyl-furan-2-carbaldehyde (1 mmol) were added to ethanol (5 ml). After 30 min 2,4-Dioxo-heptanoic acid ethyl ester (1 mmol) was added. The reaction was heated to 50° C. and stirred for 24 h. After evaporation of the solvent the residue was purified with chromatographic methods.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08278345B2 |
|---|
| Source dataset | uspto-grants-2012_10 |
|---|
| ORD ID | ord-16781ed0ff2b452ca85cfa873effc2d6 |
|---|
| Source note | uspto-grants-2012_10 |
|---|
