HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole-1-propanamine → HCID 131729978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | Baldrinal | HCID 159846 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 131729978 | HCID 131729978 | — |
Reaction Steps
Baldrinal (2) (2.7 g) was reacted with 1-(3-aminopropyl)-imidazole (2.94 g) in 2 ml of chloroform. After stirring for 10 min at room temperature, no baldrinal was detected in the reaction mixture. Compound (5) was separated on column with silica using 20:1 CHCl3:MeOH solvent system, and 26.7 mg of product was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278451B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-31900e4fcf274aeba7797ec700652a70 |
| Source note | uspto-grants-2012_10 |