HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 68538466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | Baldrinal | HCID 159846 | — |
| Product | HCID 68538466 | HCID 68538466 | — |
Reaction Steps
Baldrinal (2) (1.1 g) was reacted with octadecylamine (2.58 g) in 20 ml of chloroform. After stirring for 15 minutes at room temperature, the solution turned into thick red liquid. When all the baldrinal was reacted, an orange product (7) (53.4 mg) was collected after column chromatography on silica using 8:2 hexanes:ethyl acetate as a solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08278451B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-da00dc4dad13490a84816bbc2254d5c5 |
| Source note | uspto-grants-2012_10 |