HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86612199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Thioanisole | HCID 7520 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86612199 | HCID 86612199 | — |
Reaction Steps
Thioanisol (6.2 g, 0.05 mole) and 6.9 g (0.055 mole) of dimethyl sulfuric acid were stirred at room temperature for 12 hours. Into the reaction solution were added 100 g of water and 50 mL of diethyl ether to separate the water layer to obtain the aqueous solution of the intended dimethylphenyl sulfonium sulfate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283104B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-8bf62e7c18254e678886eaa5bca99444 |
| Source note | uspto-grants-2012_10 |