HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66916056, compound → HCID 66915943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66916056 | HCID 66916056 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66915943 | HCID 66915943 | — |
Reaction Steps
A mixture of 2-dimethylamino-6-nitro-benzenesulfonamide (753 mg, 3.07 mmol), Pd (10%) on charcoal (100 mg) and methanol (25 ml) is hydrogenated at 25° C. for 2 h. Pd is removed by filtration, the solvent evaporated and the residue crystallized from TBME/cyclohexane to give 2-amino-6-dimethylamino-benzenesulfonamide as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283356B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-be48c7d276344fcd8455744c0735d547 |
| Source note | uspto-grants-2012_10 |