HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59205146, compound → HCID 59205147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59205146 | HCID 59205146 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59205147 | HCID 59205147 | — |
Reaction Steps
30 mg of 10% Pd on carbon are added to a solution of 2-nitro-6-(2,2,2-trifluoro-ethoxy)-benzenesulfonamide (63 mg, 0.21 mmol) in EtOH (10 mL). The mixture is stirred for 30 min under hydrogen. The catalyst is removed by filtration. Evaporation of solvent gives 2-amino-6-(2,2,2-trifluoro-ethoxy)-benzenesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283356B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-f4305f5601154cbca46f0a9a0b0be780 |
| Source note | uspto-grants-2012_10 |