反应详情

A mixture of 2-fluoro-6-iodo-4-methylaniline (D1) (370 mg, 1.5 mmol), triphosgene (150 mg, 0.05 mmol), and dioxan (3 ml) was heated at reflux for 1 h 15 min then cooled and evaporated to give the crude title compound.

1. temperaturewas heated
2. temperatureat reflux for 1 h 15 min
3. temperaturethen cooled
4. customevaporated