HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59268910, compound → HCID 59268895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59268910 | HCID 59268910 | — |
| Catalyst | HCID 178479819 | HCID 178479819 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59268895 | HCID 59268895 | 32.3% |
Reaction Steps
To a solution of Grubbs I (0.345 mmol, 0.284 g) in CH2Cl2 was added diene 97 (6.91 mmol, 1.49 g). The reaction mixture was stirred at room temperature for 48 h. The reaction mixture was purified by flash chromatography (hexanes) to afford compound 98 (0.42 g, 32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283358B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-ec35891ef7e6461da92483061160a1c5 |
| Source note | uspto-grants-2012_10 |