HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium periodate → HCID 59268863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 59268872 | HCID 59268872 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59268863 | HCID 59268863 | — |
Reaction Steps
To a solution of sodium periodate (1.91 mmol, 0.41 g) in THF (3 mL) and H2O (2 mL) at 0° C. was added diol 99 (1.91 mmol, 0.42 g). The reaction mixture was stirred at room temperature for 3 h. The reaction mixture was filtered, and the resulting dialdehyde 100 was used as is, as an aqueous solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08283358B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-0a4d6b3f4dcb42b0ae68705385c38c66 |
| Source note | uspto-grants-2012_10 |