HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57650585, compound → HCID 57650511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57650585 | HCID 57650585 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 57650511 | HCID 57650511 | — |
Reaction Steps
A solution of the Boc-protected triazole product of Step C (1 g) in 40 ml of 40% TFA/DCM was stirred at room temperature for 4 h. The mixture was concentrated in vacuo and used directly as the TFA salt in the next step. MS: calculated: 290.13. Found (MH+): 291.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288371B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-a0a56f7e1f8144a393ab47782bd6b29c |
| Source note | uspto-grants-2012_10 |