HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl (2R)-2-carbamoylpyrrolidine-1-carboxylate → HCID 70894387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl (2R)-2-carbamoylpyrrolidine-1-carboxylate | HCID 6950960 | — |
| Solvent | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | HCID 70894387 | HCID 70894387 | — |
Reaction Steps
A solution of the amide from Example 33 (1.56 g, 6.28 mmol) in 10 mL of dimethylformamide dimethyl acetal was heated to 120° C. for 2 h. After cooling, the solvent was evaporated under high vacuum and the residue was taken to the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288371B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-3536c8813152440cb9496a23f3ba2820 |
| Source note | uspto-grants-2012_10 |