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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2063596Generated: October 31, 2026

Triethylamine → HCID 73320032, compound

https://huagongshe.com/reaction/2063596

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant3-MethylacetophenoneHCID 11455—
ReactantHCID 60209693HCID 60209693—
SolventEthanolHCID 702—
ProductHCID 73320032HCID 73320032—

Reaction Steps

The title compound was prepared from 4-hydrazino-2-methylquinazoline dihydrochloride (250 mg, 1.01 mmol), triethylamine (0.35 mL, 2.02 mmol) and 3-methylacetophenone (0.35 mL, 2.63 mmol) in ethanol (5 mL) by a procedure similar to Example 4, step 4 yielding 11 mg (4%) of a yellow solid. HPLC Purity: 95%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08288398B2
Source datasetuspto-grants-2012_10
ORD IDord-a659e713dfe942a69426e162dd14e154
Source noteuspto-grants-2012_10