HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 73320032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Methylacetophenone | HCID 11455 | — |
| Reactant | HCID 60209693 | HCID 60209693 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 73320032 | HCID 73320032 | — |
Reaction Steps
The title compound was prepared from 4-hydrazino-2-methylquinazoline dihydrochloride (250 mg, 1.01 mmol), triethylamine (0.35 mL, 2.02 mmol) and 3-methylacetophenone (0.35 mL, 2.63 mmol) in ethanol (5 mL) by a procedure similar to Example 4, step 4 yielding 11 mg (4%) of a yellow solid. HPLC Purity: 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-a659e713dfe942a69426e162dd14e154 |
| Source note | uspto-grants-2012_10 |