HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 57938799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-2-methylquinazoline | HCID 2785421 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57938799 | HCID 57938799 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-methylquinazoline (1.0 g, 5.6 mmol), N-methylhydrazine (0.89 mL, 16.8 mmol) and potassium carbonate (1.3 g, 22.4 mmol) in dry THF (20 mL) by a procedure similar to example 1, step 3 yielding 380 mg (36%) of a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-c280d2f41724486699ac728c0b8f3dce |
| Source note | uspto-grants-2012_10 |