HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Dimethylaminoacetophenone → (4-{1-[(6-Chloro-2-methoxy-pyrimidin-4-yl)hydrazono]-ethyl}-phenyl)-dimethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Dimethylaminoacetophenone | HCID 75037 | — |
| Reactant | (6-Chloro-2-methoxy-pyrimidin-4-yl)hydrazine | HCID 55281294 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | (4-{1-[(6-Chloro-2-methoxy-pyrimidin-4-yl)hydrazono]-ethyl}-phenyl)-dimethylamine | HCID 72577512 | — |
Reaction Steps
The title compound was prepared from (6-chloro-2-methoxy-pyrimidin-4-yl)hydrazine (414 mg, 2.4 mmol) and 4-dimethylaminoacetophenone (387 mg, 2.4 mmol) in ethanol (10 mL) by a procedure similar to Example 1, step 4 yielding 305 mg (40%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-d19008241f214c78b5ba45f3348a6f47 |
| Source note | uspto-grants-2012_10 |