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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2063609Generated: November 4, 2026

Hydrazine → HCID 60209697, compound

https://huagongshe.com/reaction/2063609

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazineHCID 9321—
ReactantSodium CarbonateHCID 10340—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 59846662HCID 59846662—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 60209697HCID 60209697—

Reaction Steps

[2-Ethyl-6-(2-methoxy-phenyl)-pyrimidin-4-yl]-hydrazine was prepared from 4-chloro-2-ethyl-6-(2-methoxy-phenyl)pyrimidine (0.91 g, 3.7 mmol), hydrazine (0.69 mL, 22 mmol), sodium carbonate (0.76 g, 7.1 mmol) and potassium carbonate (0.79 g, 5.5 mmol) in dioxane (10 mL) by a procedure similar to example 3, step 1 yielding 0.77 g (86%) of a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08288398B2
Source datasetuspto-grants-2012_10
ORD IDord-40bdab6633c241dd9a03c15667d202f9
Source noteuspto-grants-2012_10