HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → [6-(2-Methoxy-phenyl)-pyrimidin-4-yl]-hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-6-(2-methoxyphenyl)pyrimidine | HCID 15206835 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | [6-(2-Methoxy-phenyl)-pyrimidin-4-yl]-hydrazine | HCID 60209698 | — |
Reaction Steps
[6-(2-Methoxy-phenyl)-pyrimidin-4-yl]-hydrazine was prepared from 4-Chloro-6-(2-methoxy-phenyl)pyrimidine (2.4 g, 11 mmol), hydrazine (1.3 mL, 43 mmol) and potassium carbonate (2.2 g, 16 mmol) in 25 mL of dioxane by a procedure similar to example 3, step 1 yielding 2.0 g (86%) of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-62b1bcdbea6345acb3efe5914e019b3f |
| Source note | uspto-grants-2012_10 |