HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-METHYLACETOPHENONE → N-[6-(2-Methoxy-phenyl)-pyrimidin-4-yl]-N'-[1-p-tolyl-ethylidene]-hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-METHYLACETOPHENONE | HCID 8500 | — |
| Reactant | [6-(2-Methoxy-phenyl)-pyrimidin-4-yl]-hydrazine | HCID 60209698 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-[6-(2-Methoxy-phenyl)-pyrimidin-4-yl]-N'-[1-p-tolyl-ethylidene]-hydrazine | HCID 73320075 | — |
Reaction Steps
The title compound was prepared from [6-(2-methoxy-phenyl)-pyrimidin-4-yl]-hydrazine (500 mg, 2.3 mmol) and 4-methylacetophenone (310 μL, 2.3 mmol) in 10 mL of ethanol by a procedure similar to example 1, step 4 yielding 302 mg (39%) of a pale solid. HPLC Purity: 91%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-8d4b2791f958484682bded33eec596ff |
| Source note | uspto-grants-2012_10 |