HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-METHYLACETOPHENONE → HCID 73320087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-METHYLACETOPHENONE | HCID 8500 | — |
| Reactant | HCID 60209697 | HCID 60209697 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 73320087 | HCID 73320087 | — |
Reaction Steps
The title compound was prepared from [2-ethyl-6-(2-methoxy-phenyl)-pyrimidin-4-yl]-hydrazine (100 mg, 0.41 mmol) and 4-methylacetophenone (55 μL, 0.41 mmol) in 1.0 mL of ethanol by a procedure similar to example 1, step 4 yielding 117 mg (79%) of a yellow solid. HPLC Purity: 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-82a3daf4bccb4de6b6b76582c591b5cb |
| Source note | uspto-grants-2012_10 |