HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 60209701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-2-methyl-6-phenylpyrimidine | HCID 796128 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 60209701 | HCID 60209701 | — |
Reaction Steps
N-methyl-N-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine was prepared from 4-chloro-2-methyl-6-phenylpyrimidine (500 mg, 2.4 mmol), methylhydrazine (0.52 mL, 9.8 mmol) and potassium carbonate (506 mg, 3.7 mmol) in 5 mL of 1,4 dioxane by a procedure similar to example 3, step 1 yielding 392 mg (75%) of a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-2ef578fa8b9340f3ae2343743b6d6ec8 |
| Source note | uspto-grants-2012_10 |