HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-METHYLACETOPHENONE → HCID 73319790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-METHYLACETOPHENONE | HCID 8500 | — |
| Reactant | HCID 60209701 | HCID 60209701 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 73319790 | HCID 73319790 | — |
Reaction Steps
The title compound was prepared from N-methyl-N-(2-methyl-6-phenyl-pyrimidin-4-yl)-hydrazine (196 mg, 0.91 mmol) and 4-methylacetophenone (122 μL, 0.91 mmol) in 10 mL of ethanol by a procedure similar to example 8, step 4 yielding 180 mg (60%) of a cream solid. HPLC Purity: 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288398B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-3848e393c2484aaebb3f26d6483af3eb |
| Source note | uspto-grants-2012_10 |