HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-phenyl-1H-1,2,4-triazol-3-amine → 2-(4-Methyl-imidazol-1-yl)-5-(1-phenyl-1H-[1,2,4]triazol-3-ylamino)-benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-phenyl-1H-1,2,4-triazol-3-amine | HCID 21821744 | — |
| Reactant | 5-bromo-2-(4-methyl-1H-imidazol-1-yl)benzonitrile | HCID 66961517 | — |
| Product | 2-(4-Methyl-imidazol-1-yl)-5-(1-phenyl-1H-[1,2,4]triazol-3-ylamino)-benzonitrile | HCID 46214241 | — |
Reaction Steps
Prepared in analogy to example 1b) starting with 5-bromo-2-(4-methyl-imidazol-1-yl)-benzonitrile and 1-phenyl-1H-[1,2,4]triazol-3-ylamine. The title compound was obtained as a brownish solid (Yield=64%). MS ISP (m/e): 340.4 (100) [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288403B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-5d20d1131d9b4c5ba1b7b76ba4f9429b |
| Source note | uspto-grants-2012_10 |