Benzyl Bromide → 1-Benzyl-1H-[1,2,4]triazol-3-ylamine

HRID 2063659Notes

Reaction equation

HRID 2063659 reaction equation
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[CH2:7](Br)[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[CH2:7]([N:4]1[CH:5]=[N:6][C:2]([NH2:1])=[N:3]1)[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 7498Benzyl BromideHCID 178418311HCID 178418311, compound

Product 1

HCID 28409541-Benzyl-1H-[1,2,4]triazol-3-ylamine

Procedure

Prepared in analogy to example 3a) starting with 3-amino-1,2,4-triazole and benzyl bromide. The title compound was obtained as a colorless solid (Yield=14%). MS ISP (m/e): 175.3 (100) [(M+H)+].

Workup

  1. customPrepared in analogy to example 3a)

Sources & evidence

ORD record
ord-cd73df6bc4f0430bb603109b78231aa4
Source dataset
uspto-grants-2012_10
Patent number
US08288403B2

Reaction notes

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