HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2063685Generated: October 31, 2026
Ethyl bromopyruvate → HCID 59324073, compound
https://huagongshe.com/reaction/2063685
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl bromopyruvate | HCID 66144 | — |
| Reactant | [3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]thiourea | HCID 71650841 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59324073 | HCID 59324073 | 72.5% |
Reaction Steps
A suspension of [3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-thiourea (131 mg, 0.50 mmol) and ethyl bromopyruvate (74 μl, 0.50 mmol) in EtOH (3 ml) was stirred at 60° C. for 18 hours. The solid was filtered off and washed with cold EtOH, then dried in vacuo to give the title compound as light brown solid (130 mg, 72%). MS ISP (m/e): 359.1 (100) [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08288403B2 |
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| Source dataset | uspto-grants-2012_10 |
|---|
| ORD ID | ord-8d9e16be6d704d5badc96d5031c6e67f |
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| Source note | uspto-grants-2012_10 |
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