HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69122201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57423913 | HCID 57423913 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69122201 | HCID 69122201 | — |
Reaction Steps
A solution of 1,1-dimethylethyl 4-[6-(1-methylethyl)-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl]-1-piperidinecarboxylate D34 (0.71 g) in methanol (30 mL) was treated with a saturated solution of hydrogen chloride in ethanol (10 mL). The mixture was stirred for 1 hour when the solvent was removed to give the title compound as a white solid (0.59 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288413B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-96b0bcc39b394adbbcbb65b7a31714dd |
| Source note | uspto-grants-2012_10 |