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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2064070Generated: October 31, 2026

Hydrochloric Acid → HCID 69122201, compound

https://huagongshe.com/reaction/2064070

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57423913HCID 57423913—
SolventEthanolHCID 702—
SolventMethanolHCID 887—
ProductHCID 69122201HCID 69122201—

Reaction Steps

A solution of 1,1-dimethylethyl 4-[6-(1-methylethyl)-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl]-1-piperidinecarboxylate D34 (0.71 g) in methanol (30 mL) was treated with a saturated solution of hydrogen chloride in ethanol (10 mL). The mixture was stirred for 1 hour when the solvent was removed to give the title compound as a white solid (0.59 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08288413B2
Source datasetuspto-grants-2012_10
ORD IDord-96b0bcc39b394adbbcbb65b7a31714dd
Source noteuspto-grants-2012_10