HRID2064155
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1,1-Dimethylethyl 4-(6-methoxy-5-chloro-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)-1-piperidinecarboxylate (D49) (35 mg) was dissolved in ethanol (1 ml) and HCl (4M in 1,4-dioxane, 1 ml) was added at room temperature. The mixture was stirred at room temperature for 4 h then evaporated to give the title compound, 30 mg.
WORKUP
后处理
- customthen evaporated