HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylcyclohexanone → 1-(4-Methylcyclohex-1-en-1-yl)pyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylcyclohexanone | HCID 11525 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Product | 1-(4-Methylcyclohex-1-en-1-yl)pyrrolidine | HCID 11171167 | 99% |
Reaction Steps
Following the general methods as outlined under Intermediate 1, starting from 4-methylcyclohexanone, and pyrrolidine, the title compound was isolated in 99% yield (96% purity by HPLC). MS(ESI+): 166.4; MS(ESI−): 164.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288432B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-9c1808d1a6894312a4417633c257dc6c |
| Source note | uspto-grants-2012_10 |