Ethane, 2-bromo-1,1-diethoxy- → HCID 57489315, compound
Reaction equation
[CH2:1]([O:3][C:4]([C:6]1[NH:7][C:8](=[S:12])[NH:9][C:10]=1[CH3:11])=[O:5])[CH3:2].[CH2:13]([O:15][CH:16]([O:19][CH2:20][CH3:21])[CH2:17]Br)[CH3:14]>>[CH2:1]([O:3][C:4]([C:6]1[N:7]=[C:8]([S:12][CH2:17][CH:16]([O:19][CH2:20][CH3:21])[O:15][CH2:13][CH3:14])[NH:9][C:10]=1[CH3:11])=[O:5])[CH3:2]Participants
3
Procedure
prepared by reaction of 5-methyl-2-thioxo-2,3-dihydro-1H-imidazole-4-carboxylic acid ethyl ester with bromoacetaldehyde diethyl acetal. LC-MS: tR=0.70 min; [M+H]+=303.4.
Sources & evidence
- ORD record
- ord-3f42952cceac4917989f7f59470b2421
- Source dataset
- uspto-grants-2012_10
- Patent number
- US08288435B2
Reaction notes
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