D-Phenylalanine → Dl-Phenylalanine

HRID 2065589Notes

Reaction equation

HRID 2065589 reaction equation
[C:1]([C@H:4]([NH:12]C1C(C(O)=O)=CC2C(=CC=C(Cl)C=2)N=1)[CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)([OH:3])=[O:2].N[C@@H](C(O)=O)CC1C=CC=CC=1>>[NH2:12][CH:4]([C:1]([OH:3])=[O:2])[CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 71567D-PhenylalanineHCID 45256876HCID 45256876, compound

Product 1

HCID 994Dl-Phenylalanine

Procedure

Analysis of the sample enriched by (2%) substance obtained according to the procedure described in Example 6 (2-((R)-1-Carboxy-2-phenyl-ethylamino)-6-chloro-quinoline-3-carboxylic acid, obtained using D-phenylalanine as a starting material) resulted in an increase of peak with Rt 39.32 min.

Workup

  1. customAnalysis of the sample enriched by (2%) substance obtained
  2. customobtained
  3. customresulted in
  4. temperaturean increase of peak with Rt 39.32 min.

Sources & evidence

ORD record
ord-78902ca8184c412faa777da9987b6ee0
Source dataset
uspto-grants-2012_10
Patent number
US08288549B2

Reaction notes

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